Volatile organic compounds results, Mar 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATAX 0 2MARO 6X05156.D Vial: 9 Acq On 6 Mar 2002 7:31 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 3 Ethane, isocyano- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

20.70 0.05 ug/L 34372 CHLOROBENZENE-D5 21.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, isocyano- 55 C3H5N 000624-79-3 3 2 Butane, l-bromo-4-chloro- 170 C4H8BrCl 006940-78-9 2 3 Hexane, l-chloro-5-methyl- 134 C7H15C1 033240-56-1 1 4 Silanamine, N-silyl- 77 H7NSi2 _______ 005702-11-4 1 Abundance Scan 983 (20.704 min): 05156.D (-) m/z 55.05 100.00% 55 91 41

5000 77

20.40 20.60 20.80 21.00 m/z 91.10 83.79% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #70: Ethane, isocyano- 29 55

5000 20.40 20.60 20.80 21.00 40 m/z 41.05 64.66% / 15 ■ ■ i ■ “ ' i ■' -H— Tp 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ " i ■ ■ ■ ■ r ■ " i ■ ■ ■' i ■ ■ ■ ■ i ■'

m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #68172: Butane, 1-bromo-4-chloro- 55 91 20.40 20.60 20.80 21.00 5000 m/z 77.10 41.07% 27

............. II 35........ 1 ku ' ‘ 11 ‘ " I''1 ■ i' " ' I' ■' ' I ‘ ■ ■ ।।■ 11. 1... ।. ।107 134 ,'i'|.।।I" "I■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 ' Abundance #6105: Hexane, 1-chloro-5-methyl- . .................................. 91 20.40 20.60 20.80 21.00 m/z 93.10 N 26.55% 55

5000 42 27 83 i 1..... 70 ■' i"1 ■ i" ■ ■ i ■ ■" i [ | -mpmmppmtp -n-p-n-r-p-T T-p-m-p-r ■ I ■ ■ ‘ m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 20.40 20.60 20.80 21.00

05156.D HP022702.M Thu Mar 07 08:55:27 2002 Page 3

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