VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02feb15\03015.D Vial: 12 Acq On : 15 Feb 2002 5:48 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Methoxyacetonitrile Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

19.29 0.04 ug/L 35940 CHLOROBENZENE-D5 21.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methoxyacetonitrile 71 C3H5NO 001738-36-9 3 2 1-Butanol 74 C4H10O 000071-36-3 2 3 1,6-Heptadien-4-ol 112 C7H12O 002883-45-6 2 4 Acetaldehyde 44 C2H40 000075-07-0 2 Abundance Scan 885 (19.291 min): 03015.D (-) m/z 43.05.100.00% 48 8000 71 6000

4000 19.00 19.20 19.40 19.60 ।" " i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■' । ■1 ■11" ■ ■ i ■ ■ ■ ■ । ■ i ■1 ■ ■ । । । ■1 ■11 ■ ■ • ■ । <•।>••>।•••■। • m/z 1.05 73.68% m/z->___ 5 10 15 20 25 30. 35 . 40 45 50 55 60. 65. 70 75 80 85 Abundance ~ #240: Methoxyacetonitrile 41 29

1 ■ i ■ 5000 70 ■ 1 i ' ■ ■ ■ i ■ ■ 19.00 19.20 19.40 19.60 15 m/ Z 71.05 67.12% 26 38 44 54 . i 111! i 111 p i n p i ******/****[* -p-n-rp-rTT N mfa-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 Abundance 31 41 56 ' ' I ' ' ' ' i 1 1 27 19.00 19.20 19.40 19.60 5000 m/z 44.05 24.64% 44 38 73 111s1tt4at11111141441144111dd1-dAd1Ass**** m/z->___ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 Abundance #2591:1,6-Heptadien-4-ol 43 19.00 19.20 19.40 19.60 71 5000 27

m/z-> I‘ 5 ‘' I' '' 'I"' 'I ""I ' 10 15 20 25 31 " i1"' i" " i ■ 30 35 +PTT 53 40 45 50 55 60 65 -94+-79-m7 70 75 80 85

03015.D HP021302.M Fri Feb 15 18:28:40 2002 Page 4

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