Volatile organic compounds blank results, Mar 1 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02MAR01\04036F.D Vial: 29 Acq On : 2 Mar 2002 9:23 am Operator: Sample : nyc fb Inst : 210 Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Hexane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

9.85 0.63 ug/L 200806 1,4-DIFLUOROBENZENE 15.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane 86 C6H14 000110-54-3 50 2 3-Buten-l-ol, 3-methyl- 86 C5H10O 000763-32-6 47 3 1-Butanol 74 C4H10O 000071-36-3 40 4 Pentane, 2,4-dimethyl- 100 C7H16 000108-08-7 38 Abundance Scan 595 (9.850 mln): 04036F.D (-) m/z 57.1b 100.00% 57 41 5000

67 j1 91 86 , 9.60 2 9.80 10.00 10.20 51 41.05 64.30% “ i ■ ■ ■■ i ■" ■i■■ ■ ■ i ■ ■' ■ i ■ ■ ■■ i • ■ •■i Ht* *um—*umeaup—anmgumuEm m/Z m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #736: Hexane 57 43 29 5000 . 9.60 9.80 10.00 10.20 m/z 43.1b 57.61% 15 86

m/z—> - i" " i ■" ■ i PmPmmmmmp 71 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m mH Abundance #71 9:3-Buten-1-ol, 3-methyl- 41 56

31 68 . 9.60 9.80 10.00 10'20 5000 m/z 56.05 50.79%

86

m/z—> 5 ’ ’111 ’ ’ ’111’7741 TT +1“ i1 " I " “ 1 " ‘' i' ‘ " I ‘ TI1 । ■i 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1124..... . T1

Abundance #62584:1-Butanol 41 56 . 9.60 9.80 10.00 10.20 m/z 42 .05 31.12%

5000-

m/z—> i ■ ■■ ■ i" " i ■ ■ ■•■ i ■ ■ ■ ■ t ■ ■ ■■ i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 + ।111■ ■ ■ ■ i‘'1 ■ I"111"i" "i■"■ i""i p AMPM I Am 9.60 9.80 44 10.00 10.20

04036F.D HP021102.M Wed Mar 06 10:04:18 2002 Page 3

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