Volatile organic compounds results, Mar 4 2002

NYC 9/11 Public Portal Document w Uat • Uiitt ACL • 4

Data File C:\HPCHEM\l\DATA\02MAR04\04512.D Vial: 20 Acq On 4 Mar 2002 11:55 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 2 Ethanamine, N-methyl-N-nitroso Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.73 0.03 ug/L 23395 1,4-DIFLUOROBENZENE 15.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 1,2-Hydraz inedicarboxaldehyde 88 C2H4N202! 000628-36-4 3 3 1,4-Dioxane 88 C4H802 000123-91-1 3 4 Propane, 1-ethoxy- 88 C5H120 ______ 000628-32-0 3 Abundance Scan 690 (15.732 min): 04512.D (-) m/z 114.05 100.00%l 1 4

5000 63 88 1 ' "I‘ '"I 15.40 15.60 15.80 16.00 44 m/z 62.95 31.43% ‘ ‘ i ■ ‘ ‘' i ‘ ‘ ■ i 11 1 1 i ■ ■ ‘ ■ I ‘ ■ i ' • ‘ ' i ‘ ‘ • i ‘ ■ I • • • * ।1 ‘ • i * m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 15.40 15.60 15.80 16.00 56 m/z 88.00 28.05

m/z-> ■ ‘ i ■ ■ ■ ■ i ■ ■ ■ • i ■1 ■ ■ i 10 20 MiL.... 73... ■I1■■ ■ i ‘ ■ ■ ■ i ■ ■ 30 40 50 60 70 80 90 100 110 120 i ■ ■ ■ • i ■' ■ ■ i' ■' ‘ i' ‘

Abundance #62891:1,2-Hydrazinedicarboxaldehyde 31 ■' i ■ ■ ■ ■ i • 1 ' ' i ■ ■ ■1 I 1 ■ ■ ■ i 15.40 15.60 15.80 16.00 5000 m/z 43.95 4.10% 60 88 wWWWWWy m/z-> 10 4 16

20 30 40 50 60 70 80 ■ • i ■ • ■ ■ i ■ • i'| i i j i । i i i j p-i i ryi i 90 100 110 120 Abundance #794: 1,4-Dioxane 29 88 15.40 15.60 15.80 16.00

58

5000 15

- I.. .45..., i ‘ ' i • ■ ■ ■ i ■ ■ /z-> 10 20 30 40 50 60 70 80 90 100 110 120

04512.D HP022702.M Tue Mar 05 09:07:06 2002 Page 2

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