Volatile organic compounds results, Mar 4 2002

NYC 9/11 Public Portal Document Llprary earcr compound KCpOLL

Data File C:\HPCHEM\l\DATA\02MAR04\04387.D Vial: 14 Acq On 4 Mar 2002 7:35 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 2 Sulfide, allyl methyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 20927 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 2 1,2-Hydrazinedicarboxaldehyde 88 C2H4N202! 000628-36-4 3 3 Propanoic acid, 2-methyl- 88 C4H802 000079-31-2 3 4 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 Abundance Scan 691 (15.749 min): 04387.D (-) m/z 114.15 100.00% 1 4

5000

63 88 15.40 15.60 15.80 16.00 ' i ■ ■ ■ ■ i' ■ ■ ■ i ■ ■ ■' i ■ ‘ ‘ i ■ • ■ ■ i ■ ■ 1' i ■ ■ ‘ ■ i ■ ' m/z 88.00 20.30% i'' ■ ■ i ■ ■ ■ ■ i ■ /z-> 10 20 30 40 50 60 70 90 80 100 110 120 Abundance #62927: Sulfide, allyl methyl 4|1

73 88 5000 T-p-n-r-p-r ‘ I ‘ ‘ ‘ I ' ' ‘ ‘ I ' 15.40 15.60 15.80 16.00 m/z 63.05 18.66% 61

m/z-> ' I ' ' ' ' 1 ' ‘ ‘ ' I ' ' ‘ ‘ I ' 10 2030405060 70 8090 100 R 110 120 Abundance #62891: 1,2-Hydrazinedicarboxaldehyde 31

1 I " " I 1 ' 1111111/11611 15.40 15.60 15.80 16.00 5000 m/z 44.00 5.50% 60 88 PMMWwAw m/z-> Abundance laho 10 16

20 30 40 45 50 60 TT-pn-n-p-r 90 #816: Propanoic acid, 2-methyl- 70 80 i' ■ ■ ■ i ■ ■ ■1 i' ■ ■ ■ i' ■ 100 110 120

43 15.40 15.60 15.80 16.00

5000 27 73 88

/z-> -rmtlz.+— 10 20 30 40 50 60 ' , . p ... 11।p 70 80 90 100 110 ।. 120

04387.D HP022702.M Tue Mar 05 08:53:27 2002 Page 2

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