Volatile organic compounds results, Mar 7 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\02mar07\5169. D Vial: 18 Acq On 7 Mar 2002 11:44 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Sulfide, allyl methyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.72 0.03 ug/L 24824 1,4-DIFLUOROBENZENE 15.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 2 1,2-Hydrazinedicarboxaldehyde 88 C2H4N2021 000628-36-4 3 3 Propanoic acid, 2-methyl- 88 C4H802 000079-31-2 3 4 1-(Propenylthio)prop-l-ene 114 C6H10S _______ 000000-00-0 3 Abundance Scan 689 (15.715 min): 5169.D (-) m/z 114.05 100.00% 1 4

5000 63 88 y... l\____ 15.40 15.60 15.80 16.00 44 m/z 63.05 28.64% • i ' ■ ‘ ■ i ■ ‘ 1' i ‘ ‘ ' i ' ‘ ‘ ■ i ■ ■ ■ ■ i ‘ ' ■ i ■ ‘ ‘ i ‘ m/z--> 10 20 30 40 50 60 70 80 90 .100 110 120 Abundance #62927: Sulfide, allyl methyl 41

73 88 5000 15.40 15.60 15.80 16.00 m/z 88.00 21.40% 61

m/z-> ■i'■‘■i■■■■i ■ ■ ' ‘ I’ 10 20 30 48 i ■ i ■ ■ ■ ■ i • ■'' i ■ 40 50 60 70 80 90 100 110 120 Abundance #781:1,2-Hydrazinedicarboxaldehyde 31 -n-p-n-r-p- " I 1 ' “ I ‘ “ f 60 15.40 15.60 15.80 16.00 88 5000 m/z 43.95 6.11%

17 44 -MAwWwwA ...... | m/z-> 10 20 30 nanldnagan 40 50 60 70 80 90 ■' i ■ ■ ■ ■ i ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' 100 110 120 Abundance #816: Propanoic acid, 2-methyl- 43 15.40 15.60 15.80 16,00

5000 27 73 88

m/z-> 10 20 l apaaga 30 40 50 60 70 80 90 100 110 120

5169.D HP022702.M Fri Mar 08 00:23:29 2002 Page 1

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