VOC analysis results, sample AE03934, Feb 27 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB2 7\022 7R5A.D Vial: 7 Acq On : 27 Feb 2002 1:37 pm Operator: Sample : ref 5 Inst : 210 Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Feb 28 10:33 2002 Quant Results File: HP021102.RES Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 28 10:32:40 2002 Response via : Initial Calibration DataAcq Meth : HP021102 C W Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 1088319 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 573049 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.40 152 482344 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-Dichloroethane-d4 14.63 65 259428 5.62 ug/L 0.00 Spiked Amount 5.000 Recovery = 112.40% 22) Toluene-d8 19.49 98 1382858 4.77 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.40% 50) 4-Bromofluorobenzene 26.40 95 508695 5.05 ug/L 0.02 Spiked Amount 5.000 Recovery = 101.00% Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.22 85 723648 10.06 ug/L 100 4) CHLOROMETHANE 4.83 50 725048 11.79 ug/L 100 5) VINYL CHLORIDE 4.89 62 1061658 13.87 ug/L 97 6) BROMOMETHANE 5.75 96 508647 10.23 ug/L 96 7) CHLOROETHANE 5.88 64 655077 13.59 ug/L 99 8) TRICHLOROFLUOROMETHANE 6.41 101 1078133 _ /L 100 10) 1,1-DICHLOROETHENE 7.80 61 577662 5. 70ug/L 92 11) METHYLENE CHLORIDE 8.98 49 536051 5.67 ug/L 90 12) METHYL TERT BUTYL ETHER 9.29 73 660390 5.17 ug/L 98 13) TRANS-1,2-DICHLOROETHENE 9.75 61 613180 5.93 ug/L 95 14) 1,1-DICHLOROETHANE 10.82 63 754767 6.01 ug/L 98 15) 2-BUTANONE (MEK) 12.26 43 21726 8.36 ug/L 99 16) 2,2-DICHLOROPROPANE 12.26 77 592362 6.46 ug/L 99 17) CIS-1,2-DICHLOROETHENE 12.40 61 598430 6.08 ug/L 96 18) CHLOROFORM 12.79 83 715669 5.95 ug/L 98 19) BROMOCHLOROMETHANE 13.26 49 272426 5.96 ug/L 95 20) 1,2-DICHLOROETHANE 16.91 62 302944 5.85 ug/L 98 23) 1,1,1-TRICHLOROETHANE 13.83 97 571116 5.84 ug/L 98 24) 1,1-DICHLOROPROPENE 14.24 75 614270 5.92 ug/L 99 25) CARBON TETRACHLORIDE 14.50 117 394407 5.45 ug/L 98 26) BENZENE 14.93 77 461187 5.41 ug/L 97 27) TRICHLOROETHENE 16.47 95 450213 5.58 ug/L 99 28) 1,2-DICHLOROPROPANE 16.91 63 425614 5.49 ug/L 98 29) DIBROMOMETHANE 17.68 174 128773 5.20 ug/L 93 30) BROMODICHLOROMETHANE 17.51 83 415354 5.27 ug/L 100 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 149250 5.69 ug/L 96 32) METHYL ISO-BUTYL KETONE 18.36 58 40083 3.89 ug/L 79

(#) = qualifier out of range (m) = manual integration 0227R5A.D HP021102.M Thu Feb 28 10:34:06 2002 Page 1

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