VOC analysis results, sample AE03944, Feb 20 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB20\03946.D Vial: 12 Acq On : 20 Feb 2002 5:39 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 4 Formamide Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 13.49 0.09 ug/L 85701 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Formamide 45 CH3NO 000075-12-7 4 2 Methane, nitro- 61 CH3NO2 000075-52-5 3 3 1-Pentanamine 87 C5H13N 000110-58-7 3 4 Methane, nitroso- 45 CH3NO 000865-40-7 3 Abundance Scan 559 (13.485 mln): 03946.D (-) m/z 87.10 100.00% 87

61

5000 45

75 ■ ■ i ■ ■ 2 13.20 13.40 13.60 13.80 IDITTTDTTTTTTTTTTTTTT mppm TTrprrrprTT -m-ryrrn-fT m/z 61.05 69.54% m/z--> 5 10 15 20 25 30 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #40: Formamide 45

5000 ■ ■ i ■ • ‘ ■ i ■ ■ ■' i ■ ■ 13.20 13.40 13.60 13.80 29 m/z 44.95 57.36%

m/z-> ,... 15.... Ia, rdl | > ■ I ■ | 11 > | | > > > > | ■ > < i [ i i > i | > > > । | i ■ < i | ■ H l | ■ > i ■ |

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62367: Methane, nitro- 30 T-n-p-r-np 13.20 13.40 13.60 13.80 15 61 m/z 75.10 29.58% 5000 46

m/z-> mmrHltrop—?f.. mp24mmop 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ...|.n,।.11।....p.

Abundance #62890:1-Pentanamine ■ ■ I 11 ■ ■ i 30 13.20 13.40 13.60 13.80 m/z 47.05 17.70% \ A 5000

HpTpI . (.... ।... ■,.... ।. 11. ।. i.. 41.45 5559 73 87 ________ T-p-m-p-r *’1*41 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 13.20 13.40 13.60 13.80

03946.D HP021702.M Fri Feb 22 09:29:59 2002 Page 4

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