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VOC analysis results, sample AE03015, Feb 15 2002

Machine-extracted title · confidence 95%

Laboratory results for volatile organic compounds in sample AE03015 analyzed on February 15, 2002.

NYC-WTC_000019799–000019979

Folder label: “524 2/15/02 - 2/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ 0 2 f ebl 5 \ 0 3 019. D Vial: 15 Acq On : 15 Feb 2002 7:58 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-(Propenylthio)prop-1-ene Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

15.77 0.04 ug/L 28825 1,4-DIFLUOROBENZENE 15.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2 006843-45-4 3 3 2,4,5-Trioxoimidazolidine 114 C3H2N203 000120-89-8 2 4 3-Cyclobutene-1,2-dione, 3,4-dihydr 114 C4H204 ___ 002892-51-5 2 Abundance Scan 683 (15.775 min): 03019.D (-) m/ z 114.1 £ 100.00% 1 4

5000

50 63 88 W. 15.40 15.60 15.80 16.00 16.20 m/z-2__ .. 44.111 i *' ‘ • l l’ ’’’’’1’12714E71 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 111111111/117111/7711 m/z 88.1,0 A 29.59% Abundance ~ #2940:1-(Propenylthio)prop-1-ene 41 1 4 99 45

5000 15'40 15.60 15'80 16.00 16.20 73 85 m/z 63.0 25.45% .. ... ....... J.. .... I,.. m/z->___ 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 Abundance 114 T T T TIT 15.40 15.60 15.80 16.00 16.20 58 5000 m/z 50.1,5 17.85% 86 42 71 1 ■'■ r■ ■' 1 “1'0■1 ■ 111111■"' 1""I■"' 1 ■"■ 1 ■ ■■ ■ 1"■ ■ r■ "r■ ■ ■ i■ • ■ ■ r■" i"i■ ■'■ 1 ■■ ■ ■ 1"'• 1 m/z35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 Abundance #2824:2,4,5-Trioxoimidazolidine T-p-r-n-p-r pr-T-r-r-p-T-r-p-r 43 15.40 15.60 15.80 16.00 16.20 /z 43.95 3.51% 114 5000 86

70 m/z-> -rrrprrrp mM 35 40 45 50 55 6065 70 75 80 85 90 95 100 105 110 115 120 ' ‘' I'''' I ‘ ‘ I'' " I' “ ' I " I‘ 'I‘ 'I 15.40 15.60 15.80 16.00 16.20

03019.D HP021302.M Fri Feb 15 20:38:31 2002 Page 4

NYC-WTC_000019859

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NYC-WTC_000019859Source: NYC Law Department, mirrored locally

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