VOC analysis results, sample AE02089, Feb 7 2002

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Laboratory results for volatile organic compounds in sample AE02089 analyzed on February 7, 2002.

NYC-WTC_000019422–000019569

Folder label: “524 2/6/02 - 2/7/02”

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NYC 9/11 Public Portal Document -im Library Search Compound Report -tie

-= Data File C:\HPCHEM\l\DATA\02feb06\2380 .D Vial: 8 Acq On 6 Feb 2002 9:34 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins — Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-(Propenylthio)prop-l-ene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.77 0.05 ug/L 52644 1,4-DIFLUOROBENZENE 15.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2 006843-45-4 3 3 3-Cyclobutene-1,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 4 2,3-Dioxabicyclo[2.2.2]octane 114 C6H10O2 000000-00-0 2 Abundance Scan 683 (15.774 min): 2380.D (-) m/z 114.15 100.00% = 1 4

5000 63 50 88 ■ ■ i ■ 1 ■ ■ i ' 37 43 I 57 15.40 15.60 15.80 16.00 16.20 ----- I _ i ■ 1 ■ I ■ 1 1 ' i ■ m/z 62.95 26.93% ■ ■ i ■ • ■ ■ i 1 ■ ■ ■ i ' '

miz—> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2940:1-(Propenylthio)prop-1-ene 41 1 4 99

................. / I....................... 5000 15.40 15.60 15.80 16.00 16.20 m/ Z 88.00 21.06% 59 73 85 A 47 i ■ ■ ■‘ i■ ■■ ■ i‘ ■ —1 i ‘ I • i ■ . ■. ,111... 1... ’ ■ I 1 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64088:2,4-Imidazolidinedione, 3-methyl- 1 4

15.40 15.60 15.80 16.00 16.20 58 m/z 50.05 17.79% 5000

86 42 71 n-r-r-r-r-p-r-r-r-p-r i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • > i * ■ n/z—> 20 30 40 50 60 70 90 80 100 110 120 Abundance #64087:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 58 15.40 15.60 15.80 16.00 16.20 m/z 57.15 11.80%

z—> 5000

.I -p—r-r-p-r-r ‘ 20 30 40 41 ‘ ' I ‘ ' 50 60 i ‘ 68' i ■ ‘ ■ ■ i ■ ‘ 861 ‘ i ‘ 70 80 90 ' i ‘ ‘ 100 114

' i ' 110 ’ 120 ' J 15.40 15.60 15.80 16.00 16.20

2380.D HP013102.M Wed Feb 06 22:14:06 2002 Page 3

NYC-WTC_000019503

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