VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02feb06\2093F.D Vial: 15 — Acq On 7 Feb 2002 4:48 am Operator: 201-wb — Sample fb Inst : GC/MS Ins — Misc : Multiplr: 1,00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butanoic acid, methyl ester Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. mmit 16.54 0.06 ug/L 66902 1,4-DIFLUOROBENZENE 15.13 —

Hit# of 5 Tentative ID MW MolForm CAS# Qual—

1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 83 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 3-Pyrrolidinol 87 C4H9NO 040499-83-0 7 4 Azetidine, 2-methyl- 71 C4H9N 019812-49-8 5 Abundance Scan 727 (16.541 min): 2093F.D (-) m/ z 100.00% 43 74 oot

5000 59 87 A 16.20 16.40 16.60 16.80 ■ • i ■ ■ ‘ ■ i ■

' 1 I ' ' * ' I ' * 1 ' 1 1 ' ' ' I 1Innnnnn/n/I/T ■ ■ i ■ • ■ ■ i ‘ ■ i ■ ■ ■ ' i m/z 74.05 85.28% niz-> 10 20 30 40 50 60 80 70 90 100 110 Abundance #63490: Butanoic acid, methyl ester 43 74

5000 27 ■ ■ i ■ ■ 1 1 i 1 ■ ■ • i ■ ■ ' 1 i ■ 1 ■ ■ i ■ 16.20 16.40 16.60 16.80 59 87 m/z 71.05 68.20% 37 | 102 • • i - * ‘ i ■ ■ ■ • i ■ ■ i I1 - ' I ■ ■ ■ TIt 1111111 a i iz-> 10 20 30 40 50 7060 80 90 100 110 Abundance #763:1-Butanamine, 3-methyl- 3)

16.20 16.40 16.60 16.80 5000 m/z 41.05 57.53%

15 L ■■'"r 41 55 70 87 I 1 । ‘ ' | 1 1*rn | i i i > f > r-r> । ■ rd । i i ■ > । i i i i । ■ niz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #752:3-Pyrrolidinol T T T 11 43 16.20 16.40 16.60 16.80 m/z 39.05 37.76% 5000 87 57 68 A------ "H '‘'■■■I ■ ■ ■ ‘ i ‘ ‘ 1 ' i ■ ■ ' ■ i ‘ ■ i ■ ■ j 1 ■ ■ ■ i ■ /z—> 10 20 30 40 50 60 70 80 90 100 110 16.20 16.40 16.60 16.80

mersilin — 2093F.D HP013102.M Thu Feb 07 05:28:11 2002 Page 4 —

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