DEP document fragment, February 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02FEB05\0205R5A.D Vial: 9 Acq On : 5 Feb 2002 3:15 pm Operator: 201-wb Sample : ref 5 Inst : GC/MS Ins Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Feb 14 10:16 2002 Quant Results File: HP020502.RES

Quant Method : C:\HPCHEM\1\METHODS\HP020502.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 14 10:16:00 2002 Response via : Initial Calibration DataAcq Meth : HP013102

Compound R.T. Qlon Response Cone Unit Qvalue

35) METHYL ISO-BUTYL KETONE 17.36 58 73062 4.06 ug/L 94 36) CIS-1,3-DICHLOROPROPENE 17.88 75 579559 4.66 ug/L 99 37) TOLUENE 18.65 91 1541629 5.03 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.92 75 448307 4.63 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.31 97 259680 4.89 ug/L 99 40) TETRACHLOROETHENE 20.09 166 428460 4.95 ug/L 99 41) 1,3-DICHLOROPROPANE 19.83 76 496026 4.98 ug/L 99 42) DIBROMOCHLOROMETHANE 20.53 129 293309 4.02 ug/L 99 43) 1,2-DIBROMOETHANE 20.98 107 273500 4.60 ug/L 94 4 4) CHLOROBENZENE 21.85 112 996803 4.98 ug/L 98 45) 1,1,1,2-TETRACHLOROETHANE 21.90 131 336770 4.53 ug/L 98 46) 2-HEXANONE 19.20 43 143123 4.22 ug/L 97 4 7) ETHYLBENZENE 21.90 91 1845437 5.13 ug/L 99 48) P & M-XYLENE 22.06 106 1242272 10.30 ug/L 98 49) O-XYLENE 23.03 91 1478289 5.00 ug/L 99 50) STYRENE 23.08 104 1032609 5.01 ug/L 98 51) 1,1,2,2-TETRACHLOROETHANE 24.11 83 277927 5.27 ug/L 99 53) BROMOFORM 23.95 173 135486 3.51 ug/L 98 54) ISOPROPYLBENZENE 23.75 105 1629420 4.79 ug/L 99 55) 1,2,3-TRICHLOROPROPANE 24.44 110 83222 4.57 ug/L 95 56) N-PROPYLBENZENE 24.62 91 2071951 4.83 ug/L 99 57) BROMOBENZENE 24.86 156 410039 4.68 ug/L 97 58) 1,3,5-TRIMETHYLBENZENE 24.93 105 1415966 4.87 ug/L 97 59) 2-CHLOROTOLUENE 25.10 91 1375396 4.86 ug/L 100 60) 4-CHLOROTOLUENE 25.17 91 1209630 4.61 ug/L 98 61) TERT-BUTYLBENZENE 25.73 119 1264066 4.86 ug/L 99 62) 1,2,4-TRIMETHYLBENZENE 25.82 105 1446924 4.77 ug/L 98 63) SEC-BUTYLBENZENE 26.18 105 1776698 5.03 ug/L 99 64) P-ISOPROPYLTOLUENE 26.44 119 1419034 5.19 ug/L 98 65) 1,3-DICHLOROBENZENE 26.81 146 777440 4.93 ug/L 96 66) 1,4-DICHLOROBENZENE 27.02 146 774371 4.88 ug/L 99 67) N-BUTYLBENZENE 27.33 91 1463104 5.19 ug/L 98 68) 1,2-DICHLOROBENZENE 27.87 146 665934 4.83 ug/L 99 69) l,2-DIBROMO-3-CHLOROPROPAN 29.66 157 33947 3.42 ug/L 91 70) 1,2,4-TRICHLOROBENZENE 31.96 180 429198 4.77 ug/L 97 71) HEXACHLOROBUTADIENE 32.27 225 218780 5.11 ug/L 96 72) NAPHTHALENE 32.80 1'28 565204 4.57 ug/L 99 73) 1,2,3-TRICHLOROBENZENE 33.51 180 343688 4.76 ug/L 99 74) NITROBENZENE 29.87 77 113653 29.28 ug/L 98

(#) = qualifier out of range (m) = manual integration 0205R5A.D HP020502.M Thu Feb 14 10:17:20 2002 Page 2

NYC-WTC_000019344