SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB04\01936.D Vial: 7 Acq On : 4 Feb 2002 2:17 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propenal, 3-(dimethylamino)- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

32.88 0.04 ug/L 36940 1,4-DICHLOROBENZENE-D4 27.00

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(dimethylamino)-2-(me 128 C6H12N2O 049582-62-9 2 2 3-Isothiazolecarboxamide 128 C4H4N2OS 024342-43-6 2 3 5-Isothiazolecarboxamide 128 C4H4N20S 003683-98-5 2 4 2-Butenediamide, 2-methyl-, (Z)- 128 C5H8N2O2 041138-17-4 1 Abundance Scan 1666 (32.884 min): 01936.D (-) m/z 128.15 100.00% 128

5000 • ■ ■ । ■ ■ ■ ■ । ■ i 40 51 32.60 32.80 33.00 33.20 ....11. 0 m/z 39.95 16.86% miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #4886:2-Propenal, 3-(dimethylamino)-2-(methylamino)- N A V

12.8 42

5000- 83 1 Y ' v' I , JI! II 58 111 32.60 32.80 33.00 33.20 m/z 43.15 16.76% 72 ' ■ ■ ■ i ' ■ i ' ' I1........1 ■ ■ . | ■ ■ । 98 ■ 1'i ■ ' ' i ' ' ' ■ i ' ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #4835:3-lsothiazolecarboxamide 12.8 ' ' I ‘ ‘ ' I ' ' ‘ ‘ l * ' .

85 32.60 32.80 33.00 33.20 5000 m/z 51.05 16.76% 44 112 58

miz-> 30 ■ ■ । 40 15 50 ■ 60 ■ ■ i 1 1 i ■ ■ ■ ■ i ■ ' ' ■ 70 80 i ■ 90 100 ' 100 ' I ‘ ‘ ‘ ' I ' ' ' ' I 110 120 130 Abundance #4834:5-lsothiazolecarboxamide 12.8 32.60 32.80 33.00 33.20 112 m/z 43.95 6.97% WVAWMW 5000 57 44 84

miz-> 30 .....40 I"!50... lp 60 .. 70/ 80 90 100 110 120 130 32.60 32.80 33.00 33.20

01936.D HP013102.M Wed Feb 13 10:37:29 2002 Page 5

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