SB1524 volatile analysis results, sample AEO1636, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02JAN31\1636.D Vial: 17 Acq On : 31 Jan 2002 9:24 pm Operator: 206-bh Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Titanium, [ (1,2,3-.eta.)-2-but Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.14 0.41 ug/L 38213 1,4-DIFLUOROBENZENE 14.41 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Titanium, [(1,2,3-.eta.)-2-butenyl] 207 C12H15T1 039015-02-6 74 2 Propanedinitrile, (2-methylpropylid 120 C7H8N2 013134-03-7 64 3 1,3,4-Hexatriene, 3 -methoxy- 110 C7H10O 053783-88-3 50 4cis-Bicyclo[4.2.0]octa-3,7-diene 106 C8H10 _____ 103148-59-0 28 Abundance Scan 126 (5.143 min): 1636.D (-) m/z 49.10 100.00% 49 78

63 207 5000

■ ■ 1 ■ ■ ■ "i 1 1 1 1 r 1 1 1 1 i 1 1 1 1 । ' 4.80 5.00 5.20 5.40 0 ’ ’ I" ’1’11 m/z 78.10 81.22% /z—> 2030405060 70 8090 100110120130140150160170180190200210 Abundance #24592: Titanium, K1,2,3-.eta.)-2-butenylK.eta.8-1 ,3,5,7- 39 78 104 152 2(17

5000 48 113 126 ArYyyWA 480 5.00 5.20 5.40 ‘ m/z 45.00 56.41% 0- <|i>■ 1111 i 11 ■ T 4 I'm I j»t» TTTng ‘‘"I" Tp-m-p-m- i • i । 11 > > 11 i i I | 11111 t I I 1111 11 iz-> :20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance> #3745: Propanedinitrile, (2-methylpropylidene)- 42 105 4.80 5.00 5.20 5.40 5000 78 m/z 63.10 51.24% 27 93 51 66 119

0 1888838483 ’ 11 79 mmhg TTTTYTTTTyTTTTJTTTTpTTTTyTTTTYTTTrjTTTTyTTTT miz-> 2030405060 70 8090 100110120130140150160170180190200210 Abundance #2297:1,3,4-Hexatriene, 3-methoxy- Tit T 45 4.80 5.00 5.20 5.40 77 m/z 77.10 50.54%

5000 95 67 110

0 11 »i» J4 n 111»11 ’ ’1’1414444 * • i * ■ • ■ j • ■ ■ ■ i • ■ ■ i i • » ■ • l ■ n/z—> 2030405060 70 8090 100110120130140150160170180190200210 4.80 5.00 5.20 5.40

1636.D MDLVOA.M Tue Feb 19 16:43:32 2002 Page 1

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