VOC analysis results, sample AE10890, May 2002

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Data File C:\HPCHEM\l\DATA\02MAY15\10892F.D Vial: 5 Acq On 15 May 2002 4:31 pm Operator: 201-wb Sample fb Inst : GC/MS Ins Mise : Multiplr: .1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP042202.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.73 0.03 ug/L 19599 1,4-DIFLUOROBENZENE 15.07

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2 006843-45-4 3 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 2 4 2,4,5-Trioxoimidazolidine 114 C3H2N2O3 000120-89-8 2 Abundance Scan 691 (15.733 min): 10892F.D (-) m/z 114.15 100.00% 1 4

5000 63 88

15.40 15.60 15.80 16.00 44___________________ m/z 63.05 39.20% Ti/z-> Abundance 20 30 40I

41 ' ' ' ' 1 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 50 60 70 80 #2940: 1 -(Propenylthio)prop-I -ene 90 100

99 110 1 4 120 ft 5000 15.4015.60 15.8016.00 m/z 88.00 36.05% 59 73 85 47 ' I ' ' ' ' I ' ' ''■ I ' I ,,iii.... r..... I,..... L,,- •n/z-> 20 30 40 5060 70 80 90 100 110 120 Abundance #64088: 2.4-lmida2olidinedione, 3-methyl- 1 4

15.40 15.60 15.80 16.00 58 m/z 43.95 4.98% 5000

86

42 71................................................... m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64087: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 2|9 15.40 15.60 15.80 16.00 58

Blilil 114

I ' r'''' I' 41 68 ' I ' ' ' ' I ‘ 86____________ ' I ' ' I ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' •n/z-> 20 30 40 50 60 70 80 90 100 110 120

10892F.D HP042202.M Thu May 16 09:36:29 2002 Page 1

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