SB1524 volatile analysis results, sample AEO1636, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02JAN31\0131C10A.D Vial: 11 Acq On : 31 Jan 2002 5:04 pm Operator: 206-bh Sample : cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 31 17:43 2002 Quant Results File: HP013102.RES Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 31 14:25:29 2002 Response via : Initial Calibration DataAcq Meth : HP013102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 14.39 114 158295 5.00 ug/L -0.05 21) CHLOROBENZENE-D5 20.99 117 178066 5.00 ug/L -0.03 49) 1,4-DICHLOROBENZENE-D4 26.16 152 195665 5.00 ug/L -0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.61 65 96034 6.58 ug/L -0.03 Spiked Amount 5.000 Recovery = 131.60% 22) TOLUENE-D8 17.72 98 222878 4.91 ug/L -0.03 Spiked Amount 5.000 Recovery = 98.20% 52) 4-BROMOFLUOROBENZENE 23.57 174 101765 4.60 ug/L -0.03 Spiked Amount 5.000 Recovery = 92.00%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.46 85 76391 3.57ug/L 96 4) CHLOROMETHANE 4.95 50 94238 4.767 ug/L 95 5) VINYL CHLORIDE 5.13 62 174094 8.39 ug/L 99 6) BROMOMETHANE 6.04 94 63836 6.66*ug/L 97 7) CHLOROETHANE 6.17 64 63148 6.50fug/L 89 8) TRICHLOROFLUOROMETHANE 6.73 101 290475 8.88 ug/L 96 9) ACETONE 7.64 43 22603 8.93 ug/L # 85 10) 1,1-DICHLOROETHENE 7.99 61 163477 8.74 ug/L 96 11) METHYLENE CHLORIDE 8.95 49 204478 11.69 ug/L 96 12) METHYL TERT BUTYL ETHER 9.24 73 214296 9.81 ug/L 98 13) TRANS-1,2-DICHLOROETHENE 9.60 61 174585 8.91 ug/L 98 14) 1,1-DICHLOROETHANE 10.49 63 215237 9.07 ug/L 98 15) 2-BUTANONE (MEK) 11.31 43 39058 11.63 ug/L 95 16) 2,2-DICHLOROPROPANE 11.68 77 267872 9.98 ug/L 99 17) CIS-1,2-DICHLOROETHENE 11.78 96 108919 9.07 ug/L 91 18) CHLOROFORM 12.11 83 281144 10.09 ug/L 95 19) BROMOCHLOROMETHANE 12.48 49 118708 10.41 ug/L 97 20) 1,2-DICHLOROETHANE 13.81 62 235765 11.77 ug/L 99 23) 1,1,1-TRICHLOROETHANE 12.98 97 279320 9.10 ug/L 98 24) 1,1-DICHLOROPROPENE 13.32 75 187617 8.28 ug/L 95 25) CARBON TETRACHLORIDE 13.56 117 236902 9.16 ug/L 98 26) BENZENE 13.93 78 441293 8.09 ug/L 96 27) TRICHLOROETHENE 15.18 95 143304 8.95 ug/L 94 28) 1,2-DICHLOROPROPANE 15.53 63 123331 8.81 ug/L 97 29) DIBROMOMETHANE 16.18 174 39629 8.76 ug/L 92 30) BROMODICHLOROMETHANE 16.03 83 242186 10.15 ug/L 100 31) 2-CHLOROETHYL VINYL ETHER 16.54 63 42286 10.12 ug/L 98 32) Methyl iso-butyl ketone 16.61 58 21040 10.71 ug/L 84

(#) = qualifier out of range (m) = manual integration 0131C10A.D HP021102.M Wed Feb 13 15:25:55 2002 Page 1

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