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GCMS analysis results, sample AD30315, Jan 2002

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Gas chromatography-mass spectrometry analysis report for sample AD30315, completed January 9, 2002, showing unknown compounds data.

NYC-WTC_000019163–000019173

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC2101\30315.D Vial: 6 Acq On : 22 Dec 2001 11:44 am Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 10:33 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth :.GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D. 36) Fluoranthene 0.00 202 0 N.D. d 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. d 41) Benzo(a)anthracene 0.00 228 0 N.D. 42) Bis(2-ethylhexyl)phthalate 0.00 149 0 N.D. 43) Chrysene 0.00 228 0 N.D. 45) Di-n-Octylphthalate 0.00 14.9 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. . 48) Benzo(a)pyrene 37.10 252 3109 N.D. 49) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30315.D GCMS1126.M Wed Jan 02 10:33:50 2002 Page 2

NYC-WTC_000019166

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NYC-WTC_000019166Source: NYC Law Department, mirrored locally

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