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GCMS calibration results for volatile compounds, Jan 2002

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Calibration report for gas chromatography-mass spectrometry analysis of nitrosamines and chlorinated benzenes conducted on December 22, 2001.

NYC-WTC_000019040–000019043

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

User: Galos, Marie Westchester Dept of Labs & Research Date: 01/07/2002 Time: 10:22:59

Sample: AD30085 Analysis: $C1GCMS CALIGCMS Units: ug Started: 12/22/20 00:07 Ended: 12/22/20 00:07 Analyst: MG Result source: m:\instruments\209\data\dec2101\cal40a.d\cal4Oa.rr Page: 1

Component Name Viol Result MDL n Nates odimetnyamine 45___ 2.0 2 bis(2-Chloroethyl)ether 44___ 2.0 3 1,4-Dichlorobenzene 1,3-Dichlorobenzene 38. 2.0 2.0 45 1,2-Dichlorobenzene 38” 38 2.0 6 2,2‘-oxybis( 1 -Chloropropane) 50 2.0 7 Hexachloroethane n-Nitrosodi-n-propylamine 49 2.0 8 43 47 2.0 9 10 Nitrobenzene Isophorone 45 2.0 2.0 11 bis(2-Chloroethoxy)methane 43_ 2.0 12 1,2,4-T richlorobenzene 18 2.0 13 14 Naphthalene Hexachlorobutadiene '38 . 39 2.0 2.0 exachlorocyclopentadiene 18 2.0 39 2.0 ■Chloronaphthalene 17 Dimethylphthalate 19 2.0 13 2,6-Dinitrotoluene 41 2.0 19 : Acenaphthylene 19 1.0 2011 Acenaphthene ’38 . 2.0 21 2,4-Dinitrotoluene ”42 1.0 22 Diethyiphthalate 41 38 2.0 23 24 4-Chlorophenylphenylether Fluorene 37 2.0 2.0 25 Azobenzene/1 ,2-Diphenylhydraz ”48 1.0 2614-Bromophenylphenylether n-Nitrosodiphenylamine 38 1.0 27 38 ' 2.0 28 Hexa chlorobenzene 39 1.0 29 . Phenanthrene 38 36 2.0 nthracene 2.0 i-n-butylphthalate 38 2.0 luoranthene 40 35 2.0 yrene 2.0 utylbenzylphthalate 35 " ” 2.0 enzo(a)anthracene 38 2.0 is(2-Ethylhexyl)phthalate 33 2.0 hrysene 37 ” 2.0 2.0 i-n-octylphthalate 37 enzo(b)fluoranthene 39 2.0 enzo(k)fluoranthene 37 2.0 2.0 enzo(a)pyrene 38 2.0 ideno(1,2,3-cd)pyrene 39 ibenz(a,h)anthracene 39 2.0 44 Benzo(g,h,i)perylene 37 ... 2.0

NYC-WTC_0000 19040

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NYC-WTC_000019040Source: NYC Law Department, mirrored locally

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