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GC/MS calibration data for sample 30647, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sanpl e : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 1 8:47 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title •: 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1336946 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 5131844 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.57 164 2539993 20.00 ug/1 0.00 29) Phenanthrene-diO 24.98 188 3908902 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 2393152m 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1418134 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 173249 4.03 ug/mL 0.00 Spiked Amount 5.000 Recovery = 80.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.49 74 2491 N.D. 3) bis(2-Chloroethyl)ether 11.13 93 7250 N.D. 4) 1,3-Dichlorobenzene 11.59 146 5789 N.D. 5) 1,4-Dichlorobenzene 11.72 146 6814 N.D. 6) 1,2-Dichlorobenzene 12.24 146 5870 N.D. 7) 2,2'-oxybis(1-Chloropropan 12.59 45 13310 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.07 117 2286 N.D. 11) Nitrobenzene 13.30 77 223 N.D. 12) 1sophorone 14.05 82 10130 N.D. 13) bis(2-Chloroethoxy)methane 14.84 93 5505 N.D. 14) 1,2,4-Trichlorobenzene 15.18 180 4590 N.D. 15) Naphthalene 15.33 128 19954 N.D. 16) Hexachlorobutadiene 15.88 225 2921 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.90 162 9249 N.D. 20) Dimethylphthalate 20.01 163 11820 N.D. 21) 2,6-Dinitrotoluene 20.27 165 1109 N.D. 2 2) Acenaphthylene 20.11 152 11326 N.D. 2 3) Acenaphthene 20.65 153 12280 N.D. 24) 2,4-Dinitrotoluene 21.33 165 449 N.D. 25) Diethylphthalate 22.10 149 15404 N.D. 26) 4-Chlorophenyl-phenylether 22.23 204 5244 N.D. 27) Fluorene 22.21 166 11791 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.72 77 11280 N.D.

(#) = qualifier out of range (m) = manual integration 30706.D GCMS1126.M Fri Feb 01 08:47:34 2002 Page 1

NYC-WTC_000018556

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NYC-WTC_000018556Source: NYC Law Department, mirrored locally

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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