NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54
Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS
Sanpl e : GC/MS SCAN 12/18 A Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Feb 1 8:47 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title •: 209 625/TCLP calibration table
Last Update : Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 1336946 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 5131844 20.00 ug/1 -0.03
17) Acenaphthene-dl0 20.57 164 2539993 20.00 ug/1 0.00
29) Phenanthrene-diO 24.98 188 3908902 20.00 ug/1 0.00
38) Chrysene-dl2 33.02 240 2393152m 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 1418134 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 173249 4.03 ug/mL 0.00
Spiked Amount 5.000 Recovery = 80.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.49 74 2491 N.D.
3) bis(2-Chloroethyl)ether 11.13 93 7250 N.D.
4) 1,3-Dichlorobenzene 11.59 146 5789 N.D.
5) 1,4-Dichlorobenzene 11.72 146 6814 N.D.
6) 1,2-Dichlorobenzene 12.24 146 5870 N.D.
7) 2,2'-oxybis(1-Chloropropan 12.59 45 13310 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.07 117 2286 N.D.
11) Nitrobenzene 13.30 77 223 N.D.
12) 1sophorone 14.05 82 10130 N.D.
13) bis(2-Chloroethoxy)methane 14.84 93 5505 N.D.
14) 1,2,4-Trichlorobenzene 15.18 180 4590 N.D.
15) Naphthalene 15.33 128 19954 N.D.
16) Hexachlorobutadiene 15.88 225 2921 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.90 162 9249 N.D.
20) Dimethylphthalate 20.01 163 11820 N.D.
21) 2,6-Dinitrotoluene 20.27 165 1109 N.D.
2 2) Acenaphthylene 20.11 152 11326 N.D.
2 3) Acenaphthene 20.65 153 12280 N.D.
24) 2,4-Dinitrotoluene 21.33 165 449 N.D.
25) Diethylphthalate 22.10 149 15404 N.D.
26) 4-Chlorophenyl-phenylether 22.23 204 5244 N.D.
27) Fluorene 22.21 166 11791 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 22.72 77 11280 N.D.
(#) = qualifier out of range (m) = manual integration
30706.D GCMS1126.M Fri Feb 01 08:47:34 2002 Page 1
NYC-WTC_000018556
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