NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2701\30641.D Vial: 42
Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 24 14:49 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1376829 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 5306621 20.00 ug/1 -0.02
17) Acenaphthene-diO 20.56 164 2677048 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.99 188 3887168m 20.00 ug/1 0.00
38) Chrysene-dl 2 33.03 240 2443878 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 1396400 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 168389 3.94 ug/mL 0.00
Spiked Amount 5.000 Recovery = 78.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.19 74 1596 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 11.61 146 138 N.D.
5) 1,4-Dichlorobenzene 11.72 146 402 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.07 117 239 N.D.
11) Nitrobenzene 13.09 77 221 N.D.
12) Is opho rone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 15.18 180 191 N.D.
15) Naphthalene 15.34 128 2068 N.D.
16) Hexachlorobutadiene 15.89 225 211 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.28 163 2077 N.D.
21) 2,6-Dinitrotoluene 20.28 165 843 N.D.
2 2) Acenaphthylene 20.28 152 362 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.34 165 173 N.D.
25) Diethylphthalate 22.10 149 2032 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30641.D GCMS1126.M Thu Jan 24 14:50:50 2002 Page 1
NYC-WTC_000004410
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