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GCMS analysis results for sample AD30985, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 11:40 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title ;: 209 625/TCLP calibration table Last Update ’ : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.98 178 826 N.D. 3 4) Anthracene 24.98 178 826 N.D. 35) Di-n-butylphthalate 27.04 149 16202 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.52 149 845 N.D. 41) Benzo(a)anthracene 33.01 228 3799 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 30386 0.31 ug/1 99 43) Chrysene 33.01 228 3799 N.D. 45) Di-n-Octylphthalate 35.04 149 109 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. . 4 8) Benzo(a)pyrene 37.12 252 3766 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30985.D GCMS1126.M Fri Jan 18 11:41:10 2002 Page 2

NYC-WTC_000018265

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NYC-WTC_000018265Source: NYC Law Department, mirrored locally

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