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GCMS analysis results for sample AD30984, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.

NYC-WTC_000018248–000018261

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\DEC31O1\3O984. D Vial: 38 Acq On 2 Jan 2002 12:47 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 11:39 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.05 178 1813 N.D. 34) Anthracene 25.05 178 1813 N.D. 35) Di-n-butylphthalate 27.03 149 9494 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 29.40 202 770 N.D. 40) Butylbenzylphthalate 31.71 149 1310 N.D. 41) Benzo(a)anthracene 33.03 228 5151 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 9166 N.D. 43) Chrysene 33.03 228 5151 N.D. 45) Di-n-Octylphthalate 35.06 149 1108 N.D. 46) Benzo(b)fluoranthene 36.12 252 639 N.D. 47) Benzo(k)fluoranthene 36.12 252 757 N.D. 48) Benzo(a)pyrene 37.12 252 4408 N.D. 4 9) Indeno(1,2,3 -cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30984.D GCMS1126.M Fri Jan 18 11:40:05 2002 Page 2

NYC-WTC_000018251

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NYC-WTC_000018251Source: NYC Law Department, mirrored locally

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