NYC 9/11 Public Portal Document
4
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\DEC3101\25874.D Vial: 19
Acq On 1 Jan 2002 4:27 am Operator: 209 GALOS
Inst : GC/MS 209
Sample
Mise
gems scan 12/14a
4
Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 15 12:30 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 726829 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 2839393 20.00 ug/1 -0.02
17) Acenaphthene-dlO 20.56 164 1452335 20.00 ug/1 -0.01
2 9) Phenanthrene-dl0 24.99 188 2007422m 20.00 ug/1 0.00
38) Chrysene-dl2 33.03 240 1204505 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 685048 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 97994 4.44 ug/mL 0.00
Spiked Amount 5.000 Recovery = 88.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.34 128 677 N.D.
16) Hexachiorobutadiene 0.00 225 0 N.D.
18) Hexachiorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.13 165 382 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
25874.D GCMS0103.M Tue Jan 15 12:31:34 2002 Page 1
NYC-WTC_000017982
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