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GCMS analysis results for sample AD30357, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.

NYC-WTC_000017748–000017769

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC2701\30357.D Vial: 18 Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 5:28 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ': Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.05 178 387 N.D. 34) Anthracene 25.05 178 387 N.D. 35) Di-n-butylphthalate 27.01 149 108368 0.53 ug/1 # 98 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.71 149 4197 N.D. 41) Benzo(a)anthracene 33.02 228 3969 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 8535 N.D. 43) Chrysene 33.02 228 3969 N.D. 45) Di-n-Octylphthalate 34.96 149 177 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.12 252 4457 N.D. ' 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz (a,h) anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30357.D GCMS1126.M Mon Dec 31 12:36:54 2001 Page 2

NYC-WTC_000017751

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NYC-WTC_000017751Source: NYC Law Department, mirrored locally

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