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GCMS blank analysis results

Machine-extracted title · confidence 95%

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document “ae Library Search Compound Report ~ "Data File : C:\HPCHEM\1\DATA\JANO802\LB.D Vial: 7 Acq on : 8 Jan 2002 7:12 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE IIIS ISIS SSSI IE ISIS SOE IOEI SUISSE ISIS ISISISOTI ISO III III Peak Number 12 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 10 R.T. | EstCone Area Relative to ISTD R.T. 32.93 0.77 ug/1 210099 = Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cAS# Qual 1 3-Isopropoxy-1,241,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Ethanedioic g¢id, bis(trimethylsily 234 C8H1804Si2 018294-04-7 38 3 Trisiloxang/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 ,4_3-(3-Hydréxypheny1) -3-hydroxypropio 398 C18H3404Si3 __000000-00-0 37 Abundance ‘Scan 3038 (62.831 min): LBD) m/z 73.00 zOHOE 5000: 147 | 79. 2 = | eo seo sso0 mae | 327, 429 x i Bab, HLA 288 pelesies! w/z 147.00 43.94 miz->____80__100__180__200_250__300__350__400_450__00__550_ f oa *W60503: F-isopropoxy-1,7,1,7,7,7-hexamélhy-3,5,5-4is(timn / | 73 ee 147 . 92603280 33.00'3920 | m/z 221.0, 25.32% | attr a5 519 _ 661 ii | mz-> 60 100. 150-200 250 300 350-400-450 500.550 \ ‘Abundance i] 147 32.60 3280 33.00 3320 | 5000 m/z 281.00 18-884 : eer t s17____ 190 210 mz->____ $0100. 150 __200__250 __300__350__400__450__500__§50_ ‘Abundance ‘#74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 147 m/z 355.0, 16.32 5000. 281 45 369 417 207 249 1 mz 50 100 «150 200 250 300 360 400 450 500 550 | 32.60 32.80 33.00 33.20 i LB.D GCMS0103.M Wed Jan 09 12:34:04 2002 Page 12 NYC-WTC_000017361

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NYC-WTC_000017361Source: NYC Law Department, mirrored locally

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