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GCMS analysis log for sample AD30603

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.

NYC-WTC_000017233–000017245

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017238
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NYC 9/11 Public Portal Document om LSC Area Percent Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30603.D Vial: 31 Acq On : 28 Dec 2001 7:17 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 signal : TIC peak R.T. first max last PK peak peak peak % of # = min scan scan scan TY height area % max. total 1 7.613 276 280 293 rBV 502277 1298672 12.22% 2.289% 2 11.680 718 723 749 rBV 3148267 8106036 76.26% 14.285% 3 14.305 1002 1009 1017 rBV 110342 241095 2.27% 0.425% 4 15.278 1109 1115 1135 rBV 4212925 10174368 95.72% 17.930% 5 17.454 1346 1352 1360 rBvV 287754 618419 5.82% 1.090% 6 20.272 1653 1659 1667 rBV 214440 466053 4.38% 0.821% 7 20.566 1684 1691 1715 rBV 4482014 10629563 100.00% 18.732% 8 21.080 1740 1747 1764 rVB3 30285 142737 1.34% 0.252% 9 22.788 1927 1933 1942 rBV 140077 305575 2.87% 0.539% 10 24.982 2163 2172 2186 rBV2 4049470 10484000 98.63% 18.476% 11 26.891 2373 2380 2386 rBV 66766 139334 1.31% 0.246% 12 30.059 2720 2725 2737 rBV 521344 1139952 10.72% 2.009% 13 33.024 3041 3048 3073 rBV2 3047607 7795105 73.33% 13.737% 14 37.118 3486 3494 3515 rBV2 1654110 5204255 48.96% 9.171% Sum of corrected areas: 56745164 30603.D GCMS0103.M Thu Jan 10 15:01:15 2002 NYC-WTC_000017238

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NYC-WTC_000017238Source: NYC Law Department, mirrored locally

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