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GCMS analysis results for sample AD30633, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.

NYC-WTC_000017210–000017232

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017232
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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 28 Dec 2001 3:23 pm Data File: M:\INSTRU~1\209\DATA\DEC2701\30633.D Name: GC/MS SCAN 12/17 Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

N-Ethyl formamide 7.62 3.9 ug/1 1314680 ISTD01 11.68 6742570 20.0 Cyelotetrasiloxane, 11.13 0.5 ug/1 153263 ISTD01 11.68 6742570 20.0 Cyclopentasiloxane, 14.31 3.1 ug/1 1298100 ISTD02 15.28 8481290 20.0 1 1,1,5,7, 7,7 -Heptam 17.45 7.0 ug/1 2966410 ISTD02 15.28 8481290 20.0 2-Propanone, 1- (1-me 18.16 0.6 ug/1 256342 ISTD03 20.56 8955800 20.0 20.28 5.1 ug/1 2300070 ISTD03 20.56 8955800 20.0 Benzoic aeid, 4 - etho 21.05 0.9 ug/1 416437 ISTD03 20.56 8955800 20.0 Benzoic acid, 2,5 - bi 22.79 3.1 ug/1 1473930 ISTD04 24.99 9594220 20.0 l -Monolinoleoylglyce 26.89 1.5 ug/1 714270 ISTD04 24.99 9594220 20.0 3-Isepropoxy-1,1,1,7 28.66 1.1 ug/1 550987 ISTD04 24.99 9594220 20.0 1,1,1,5,7,7,7 -Heptam 30.25 1.5 ug/1 488372 ISTD05 33.03 6374460 20.0 Ethanedioic acid, bi 31.72 1.3 ug/1 428900 ISTD05 33.03 6374460 20.0 Ethanedioic acid, bi 34.38 1.0 ug/1 306031 ISTD05 33.03 6374460 20.0 Ethanedioic acid, bi 35.57 1.0 ug/1 195838 ISTD06 37.12 3937240 20.0 l ,11,5,7,7,7-Heptam 36.72 0.6 ug/1 114100 ISTD06 37.12 3937240 20.0

30633.D GCMS0103.M Thu Jan 10 15:24:54 2002

NYC-WTC_000017232

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NYC-WTC_000017232Source: NYC Law Department, mirrored locally

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