GCMS analysis results for sample AD30350, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30350.D Vial: 18 Acq On 1 Jan 2002 3:29 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integrat ion Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.73 1.56 ug/1 399208 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Pentanone,4- hydroxy-4-me thyl- 116 C6H1202 000123-42-2 42 2 Propanal, 2-hydroxy- 2 -methyl - 88 C4H802 020818-81-9 33 3 Acetone / 58 C3H60 000067-64-1 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance 4 Scan 293 (7.730 min): 30350.D (-) m/z 4 .05 100.00% 43

5000 59

101 —. . । , , , । i । । । । r, । । । i i i । 7.40 7.60 7.80 8.00 ------354 , 48 53., I— ———83 — i-i i । F'i‘1 m/z 59.00 47.86% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000- TpnmmmMmTfTTTTT 59 7.40 7.60 7.80 8.00 m/z 101.05 16.85% 27 ----- +49+ 1 IBoaByaa’ 83 101 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #805: Propanal. 2-hydroxy-2-methyl- 43 59 Al mmpepy 7.40 7.60 7.80 8.00 5000 31 m/z 58.05 16.22%

36 73 88 281—B—BB—E——0TTTTTTePTPTT miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone r 'I" TIPPAT 43 7.40 7.60 7.80 8.00 m/z 42.05 6.56% 5000 15 58 27 Tndr --- 1 ■ ‘ i ■ ■ । j • ■ ‘ * t ■ ■ ■ ■ i • • ■ ■ i * ‘ ‘ 1 i * * ■ • i ‘ •-12fP—PTTTMPPf miz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

30350.D GCMS1126.M Tue Jan 15 14:48:57 2002 Page 2

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