GCMS analysis results for sample AD30086, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC1901\30086.D Vial: 6 Acq On : 19 Dec 2001 2:39 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.67 ug/1 851837 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl fo:amide 73 C3H7NO 000627-45-2 9 2 Silane, to ramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxo ane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1,3-Dioxolane, 2-methyl - 88 C4H802 000497-26-7 5 Abundance Scan 279 (7.603 min): 30086.D (-) m/ z 72.9,5 100.00% 73

5000 43 87 7.20 7.40 7.60 7.80 ' 8.00 37, | , | 49 55. .61 67, t 103 ‘ ‘ l ‘ ‘ ‘ T 1 1 1 1 I ' 1 ' 1 1 111 1 11-1 1 1 1 1 1 ,l r1 Hr b i • rl 1****44 m/z 43.05 29.01% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000 i । : . . > T-i-r । । i i । । । 44 58 7.20 7.40 7.60 7.80 8.00 m/z 41.0,5 10.31% ' 15i ‘ ‘ I ‘ ‘ ’ I ‘ * —pp । ■ ■ ■ ■ । ■1' ■ । ■ ■ ■ ■ । ■ ■ ■ • । ■ ■ ■ ■ ।1 ■ • ■ । ■ ■ m/z->_____ 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane tetramethyi- 73 ITrfrrm.TTffrr 7.20 7.40 7.60 7.80 8.00 5000 m/z 45.05 10.23% 45 15 53 59 , , 88... ,,,,,,...... ‘ i ‘ ‘ ‘ i ■ ■ ' ‘ i ' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dlmet ) - TT1m T j . . . . j •-T-.-.-j l » 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.0,0 6.64% 5000

45 36 i I 55 67. +r _________________ 109115 1+1***1111sIi I1 11 । । | ' ''I ■ 'i ' 1 1 ' i ■ ■ ■ ■ i 1 rl 1 1 11 1 1 I ' 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 ' 8.00

30086.D GCMS1126.M Wed Jan 02 16:05:40 2002 Page 1

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