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GCMS analysis results for sample AD30113, Jan 2002

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GCMS analysis of environmental sample AD30113 conducted January 9, 2002.

NYC-WTC_000016717–000016725

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC19O1\3O113 .D Vial: 13 Acq On : 20 Dec 2001 1:10 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 15:50 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.98 178 1217 N.D. 3 4) Anthracene 24.98 178 1217 N.D. 35) Di-n-butylphthalate 27.00 149 22546 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 5901 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 2902 N.D. 43) Chrysene 33.02 228 5901 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.13 252 1037 N.D. 4 7) Benzo(k)fluoranthene 36.13 252 739 N.D. 48) Benzo(a)pyrene 37.11 252 4773 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30113.D GCMS1126.M Mon Dec 31 15:51:15 2001 Page 2

NYC-WTC_000016720

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NYC-WTC_000016720Source: NYC Law Department, mirrored locally

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