GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

.Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1802\31500.D Vial: 13 Acq On : 19 Jan 2002 3:19 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 14:33 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.50 152 801348 20.00 ug/1 -0.03 10) Naphthalene-d8 15.10 136 3167318 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.36 164 1587991 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.77 188 2198047 20.00 ug/1 -0.03 38) Chrysene-dl2 32.80 240 1311183 20.00 ug/1 -0.04 44) Perylene-dl2 36.86 264 834318 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 29.85 235 127306 5.05 ug/mL -0.22 Spiked Amount 5.000 Recovery = 101.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 106 N.D. 3) bis(2-Chloroethyl)ether 10.97 93 1877 N.D. 4) 1,3-Dichlorobenzene 11.42 146 904 N.D. 5) 1,4-Dichlorobenzene 11.54 146 1151 N.D. 6) 1,2-Dichlorobenzene 12.08 146 1028 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 12.88 117 178 N.D. 11) Nitrobenzene 13.25 77 1283 N.D. 12) 1sophorone 13.84 82 13466 N.D. 13) bis(2-Chloroethoxy)methane 14.54 93 3610 N.D. 14) 1,2,4-Trichlorobenzene 15.00 180 1073 N.D. 15) Naphthalene 15.15 128 5390 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.65 162 2605 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 19.97 165 185 N.D. 2 2) Acenaphthylene 19.91 152 2226 N.D. 2 3) Acenaphthene 20.45 153 2952 N.D. 24) 2,4-Dinitrotoluene 20.74 165 178 N.D. 25) Diethylphthalate 21.88 149 3871 N.D. 26) 4-Chlorophenyl-phenylether 22.01 204 1895 N.D. 27) Fluorene 21.97 166 3813 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31500.D GCMS0103.M Wed Feb 06 15:24:10 2002 Page 1

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