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GCMS analysis report, sample AD31502, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report for DEP sample AD31502 documenting analytical results from February 15, 2002.

NYC-WTC_000016593–000016602

Folder label: “GCMS X 12/31/01 A 1/18/02

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OCR text

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31502.D Vial: 8 Acq On : 18 Jan 2002 10:28 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of' largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 7.447 258 262 274 rBV 347168 907417 13.86% 2.759% 2 7.584 274 277 297 rVB2 45853 193920 2.96% 0.590% 3 11.495 698 703 722 rBV 1978945 5162434 78.86% 15.697% 4 15.094 1089 1095 1113 rBV 3110682 6373955 97.37% 19.380% 5 20.354 1662 1668 1684 rBV 3159433 6546068 100.00% 19.904%

6 24.770 2143 2149 2161 rBV2 2904429 5999845 91.66% 18.243% 7 29.847 2697 2702 2709 rBV2 334983 671421 10.26% 2.041% 8 32.803 3017 3024 3048 rBV 1798871 4188335 63.98% 12.735% 9 36.860 3459 3466 3488 rBV 1048024 2845531 43.47% 8.652%

Sum of corrected areas: 32888926

31502.D GCMS0103.M Wed Feb 06 15:36:24 2002

NYC-WTC 000016598

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NYC-WTC_000016598Source: NYC Law Department, mirrored locally

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