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GCMS unknown compounds report, sample AD31433, Feb 2002

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Laboratory report for DEP sample AD31433 identifying unknown compounds and surrogate recovery results from February 15, 2002.

NYC-WTC_000016584–000016592

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JANI802\31433.D Vial: 7 Acq On : 18 Jan 2002 9:29 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 15:15 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.84 178 218 N.D. 34) Anthracene 24.84 178 218 N.D. 35) Di-n-butylphthalate 26.79 149 7157 N.D. 36) Fluoranthene 28.46 202 180 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.31 149 803 N.D. 41) Benzo(a)anthracene 32.80 228 3925 N.D. 42) Bis(2-ethylhexyl)phthalate 33.11 149 14579 N.D. 43) Chrysene 32.87 228 1253 N.D. 45) Di-n-Octylphthalate 34.84 149 5467 N.D. 46) Benzo(b)fluoranthene 35.90 252 6808 N.D. 47) Benzo(k)fluoranthene 35.90 252 5935 N.D. 48) Benzo(a)pyrene 36.71 252 2209 N.D. 49) Indeno (1,2,3-cd) pyrene 40.45 276 281 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.52 276 921 N.D.

(#) = qualifier out of range (m) = manual integration 31433.D GCMS0103.M Wed Feb 06 15:15:44 2002 Page 2

NYC-WTC_000016587

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NYC-WTC_000016587Source: NYC Law Department, mirrored locally

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