NYC 9/11 Public Portal Document
3
1 Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\JAN1802\31433.D Vial: 7
Acq On : 18 Jan 2002 9:29 pm Operator: 209 GALOS
Sample : gc/ms scan 12/31 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 6 15:15 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Thu Dec 13 14:40:46 2001
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.50 152 750396 20.00 ug/1 -0.03
10) Naphthalene-d8 15.09 136 2918715 20.00 ug/1 -0.02
17) Acenaphthene-diO 20.35 164 1466719 20.00 ug/1 -0.03
29) Phenanthrene-diO 24.77 188 2029903 20.00 ug/1 -0.03
38) Chrysene-dl2 32.80 240 1218025 20.00 ug/1 -0.03
44) Perylene-dl2 36.86 264 779802 20.00 ug/1 -0.03
System Monitoring Compounds
37) 2,4-DDD 29.85 235 115318 4.95 ug/mL -0.22
Spiked Amount 5.000 Recovery = 99.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’-oxybi s(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.16 128 1041 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
2 0) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.81 165 183 N.D.
25) Diethylphthalate 21.88 149 1264 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
2 7) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31433.D GCMS0103.M Wed Feb 06 15:15:40 2002 Page 1
NYC-WTC_000016586
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