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GCMS analysis results for sample AD31248, Feb 25, 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31248 conducted on February 25, 2002.

NYC-WTC_000016392–000016406

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1402\31248.D Vial: 27 Acq On : 15 Feb 2002 4:25 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 11:59 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Ni trosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.76 178 304 N.D. 34) Anthracene 25.76 178 304 N.D. 35) Di-n-butylphthalate 27.72 149 4219 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.82 228 2069 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 302 N.D. 43) Chrysene 33.82 228 2160 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.11 252 2288 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31248.D GCMS0208.M Fri Feb 15 12:00:45 2002 Page 2

NYC-WTC_000016402

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NYC-WTC_000016402Source: NYC Law Department, mirrored locally

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