Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31248 conducted on February 25, 2002.
NYC-WTC_000016392–000016406Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\FEB1402\31248.D Vial: 27 Acq On : 15 Feb 2002 4:25 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 11:59 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4“Dichlorobenzene-d4 12.35 152 360431 20.00 ug/1 0.00 10) Naphthalene-dS 15.98 136 1407009 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.30 164 756557 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.75 188 1117789 20.00 ug/1 -0.02 38) Chrysene-dl2 33.82 240 796250 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 520709 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.83 235 48727 4.34 ug/mL 0.33 Spiked Amount 5.000 Recovery = 86.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.05 128 498 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.79 149 200 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31248.D GCMS0208.M Fri Feb 15 12:00:42 2002 Page 1
NYC-WTC_000016401
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