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GCMS analysis results for sample AD31401, Feb 11, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31401 conducted on February 11, 2002.

NYC-WTC_000016293–000016301

Folder label: “GCMS X 12/28/01 A 1/17/02

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Scanned page image, NYC-WTC_000016298
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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\1\DATA\JAN1602\31401.D Vial: 24 Acq On : 17 Jan 2002 10:07 am Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF. Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.446 258 262 293 rVB 424629 1229046 15.90% 3.098% 2 11.495 698 703 724 rBV 2229743 5925025 76.64% 14.935% 3 15.094 1089 1095 1113 rBV 3683799 7490611 96.89% 18.881% 4 20.354 1662 1668 1692 rBV 3528385 7731071 100.00% 19.487% 5 24.770 2143 2149 2162 rBV2 3236967 7225806 93.46% 18.214%

6 29.846 2697 2702 2709 rBV 380623 775828 10.04% 1.956% 7 32.802 3018 3024 3043 rBV2 2321169 5230623 67.66% 13.184% 8 36.869 3459 3467 3492 rBV 1432843 4064517 52.57% 10.245%

Sum of corrected areas: 39672527

31401.D GCMS0103.M Thu Feb 07 12:34:22 2002

NYC-WTC_000016298

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NYC-WTC_000016298Source: NYC Law Department, mirrored locally

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