Laboratory report of a GCMS blank run performed on February 7, 2002, to verify absence of contamination.
NYC-WTC_000016285–000016292Folder label: “GCMS X 12/28/01 A 1/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN1602\LB.D Vial: 4 Acq On : 16 Jan 2002 2:34 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS. 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 10:51 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update •: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.50 152 678002 20.00 ug/1 -0.03 10) Naphthalene-d8 15.09 136 2652651 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.35 164 1325459 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.77 188 1788146 20.00 ug/1 -0.03 38) Chrysene-dl2 32.80 240 1069878 20.00 ug/1 -0.03 44) Perylene-dl2 36.86 264 670290 20.00 ug/1 -0.03
System Monitoring Compounds 37) 2,4-DDD 29.85 235 117548 5.73 ug/mL -0.22 Spiked Amount 5.000 Recovery = 114.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 236 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. . 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'- oxybi s (l -Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.14 128 636 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enapht hene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 21.89 149 479 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS0103.M Thu Feb 07 10:51:26 2002 Page 1
NYC-WTC_000016286
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NYC-WTC_000016506
Blank analysis report for DEP sample AD31363 showing non-detect levels for volatile organic compounds from February 7, 2002.
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Blank analysis report for DEP sample AD31432 showing non-detect levels for volatile organic compounds from January 22, 2002.
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Method blank report confirming absence of contamination during volatile organic compound testing procedures in January 2002.
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Laboratory blank report confirming no detectable contamination for nitrosamines and chlorinated solvents during the run.
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Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD31434.
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Laboratory report documenting GCMS analysis of sample AD31465 conducted on February 11, 2002.
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Blank analysis report for GCMS testing of sample AE00005 showing non-detectable levels of target compounds.
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1 shared topics · similarity 0.997
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Blank analysis report showing non-detectable levels of volatile organic compounds in laboratory reagents on February 15, 2002.
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GCMS analysis results for sample AD28903 dated December 15, 2001, showing non-detect levels for various compounds.
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Laboratory data table recording drip rates and volumes for GCMS Method 508 analysis.
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Blank analysis report for DEP sample AE02966 showing all target compounds below minimum detection limits.
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