GCMS analysis summary, sample AD31375, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JANI502\31375.D Vial: 8 Acq On : 15 Jan 2002 5:47 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 4 13:59 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE.Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.50 152 735719 20.00 ug/1 -0.20 10) Naphthalene-d8 15.10 136 2880951 20.00 ug/1 -0.21 17) Acenaphthene-diO 20.36 164 1454242 20.00 ug/1 -0.22 29) Phenanthrene-diO 24.77 188 1963530 20.00 ug/1 -0.22 38) Chrysene-dl2 32.80 240 1109586 20.00 ug/1 -0.24 44) Perylene-dl2 36.86 264 707313 20.00 ug/1 -0.26

System Monitoring Compounds 37) 2,4-DDD 29.85 235 121984 5.65 ug/mL -0.22 Spiked Amount 5.000 Recovery = 113.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 194 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichiorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichiorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.16 128 1515 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.72 165 208 N.D. 25) Diethylphthalate 21.89 149 519 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31375.D GCMS1126.M Mon Feb 04 14:01:13 2002 Page 1

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