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GCMS reference standard results for organic compounds, February 2002

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Reference analysis report confirming instrument performance with measured values for nitrosamines and chlorinated solvents.

NYC-WTC_000016073–000016077

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1502\REFA.D Vial: 6 Acq On : 15 Jan 2002 2:50 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise : ■ Multiplr: 1.00 MS Integration Params: RTEINT.P 1 Quant Time: Feb 4 12:48 2002 ■ (Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon -Response Cone Unit / Qvalue

30) N-Nitrosodiphenylamine 22.40 168 97341 2.68 ug/1 98 31) 4-Bromophenyl-phenylether 23.46 248 67497 3.36 ug/1 98 32) Hexachlorobenzene 23.87 284 78377 3.54 ug/1 97 33) Phenanthrene 24.84 178 403539 3.73 ug/1 99 34) Anthracene 24.96 178 348042 3.22 ug/1 99 35) Di-n-butylphthalate 26.79 149 592988 4.12 ug/1 99 36) Fluoranthene 28.44 202 373641 3.57 ug/1 98 3 9) Pyrene 29.11 202 390387 3.79 ug/1 99 40) Butylbenzylphthalate 31.30 149 188758 3.50 ug/1 96 41) Benzo(a)anthracene 32.75 228 249318 3.50 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.11 14 9 244605 3.36 ug/1 98 43) Chrysene 32.87 228 270866 3.88 ug/1 98 45) Di-n-Octylphthalate 34.85 149 242564 2.57 ug/1 97 46) Benzo(b)fluoranthene 35.83 252 196247 3.67 ug/1 99 47) Benzo(k)fluoranthene 35.89 252 251707 4.59 ug/1 97 48) Benzo(a)pyrene 3 6.70 252 137579 2.96 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.42 276 137011 2.95 ug/1 94 50) Dibenz(a,h)anthracene 40.48 278 113787 3.13 ug/1 98 51) Benzo(g,h,i)perylene 41.47 276 132146 3.33 ug/1 96

(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Mon Feb 04 12:50:33 2002 Page 2

NYC-WTC_000016076

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NYC-WTC_000016076Source: NYC Law Department, mirrored locally

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