NYC Law Department release
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← Document results/DEP Box 15/508 X 5/10/02 5/14/02
Document / 9 pages

GCMS pesticide analysis report, sample AE10996, May 2002

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for the detection of organochlorine pesticides including Aldrin and Dieldrin.

NYC-WTC_000015854–000015862

Folder label: “508 X 5/10/02 5/14/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document yuantltation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\020514\TOXC1.D\ECD1A.CH Vial: 9 Signal #2 : C:\MSDCHEM\1\DATA\508\020514\TOXC1.D\ECD2B.CH Acq On : 14 May 2002 12:12 pm Operator: Nefliu Sample : tox CCV1 Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS2.E Quant Time: May 14 13:16:32 2002 Quant Results File: 020509T.RES

Quant Method : C:\MSDCHEM\1\METHODS\020509T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update ; Thu May 09 14:04:48 2002 Response via : Initial Calibration DataAcq Meth : 508P.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 8) s 2,4-DDD SURROGAT 13.02 13.52 919.1E6 947.9E6 0.184m 0.194m Spiked Amount 0.200 Recovery = 92.00% 97.00%

Target Compounds 1) Toxaphene 1 13.37 12.95 38440755 10836570 0.525m 0.676m# 2) Toxaphene 2 13.68 14.12 62804672 31241415 0.584m 0.569m 3) Toxaphene 3 14.15 14.45 52243706 129.3E6 0.574m 0.600m 4) Toxaphene 4 14.22 14.58 100.7E6 35871922 0.590m 0.581m 5) Toxaphene 5 14.49 14.90 36317606 116.8E6 0.601m 0.576m 6) Toxaphene 6 14.97 15.12 125.2E6 36790570 0.549m 0.575m 7) Toxaphene 7 15.31 15.73 124.4E6 133.3E6 0.545m 0.558m

2 •' ’

(g4.)

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. TOXC1.D 020509T.M Thu May 16 10:48:40 2002 Page 1

NYC-WTC_000015859

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NYC-WTC_000015859Source: NYC Law Department, mirrored locally

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