GCMS analysis report, sample AE12763, June 2002

NYC 9/11 Public Portal Document Library searen Compound Report

Data File C:\MSDCHEM\l\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Acetic acid, chloro-, ethyl... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

3.92 1.13 ug/L 963223 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 4/ 2 Ethyl Chloride 64 C2H5C1 000075-00-3 2 3 1-Propanol, 3-chloro- 94 C3H7C1O 000627-30-5/1 4 Borane, trifluoro- 68 BF3 007637-07-/ 1 Abundance Scan 143 (3,919 min): 12763.D (-141) (-) m/z 49.10 100.00% 49

5000

miz-> O+ -411 10 20 30 40 50 7 m/z 3.60 3.80 51.05 4.00 4.20 20.45% 60 70 80 90 100 110 120 130 Abundance #108005: Acetic acid, chloro-, ethyl ester 23

5000 ‘ 1 ‘ I ‘ ‘ 1 ‘ ‘ ■ I ‘ ‘ I ' ' ' ‘ I

77 3.60 3.80 4.00 4.20 42 49 m/z 48.00 12.97% 14 | 88 94 107 122 miz-> 0! - 10 20 30 35 1*4’4 l'1 40 10,1/111.59.65.) 50 60 70 80 ■111 ■ ■ ■ ■ p i'i ■ p ■ •’■ i .... p ... p

90 100 110 120 130 Abundance #107943: Ethyl Chloride 23 3.60 3.80 4.00 4.20 64 5000 m/z 35.10 7.06% / 49 35 15 -H I iz-> Of 10 +— t——t 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #108340:1-Propanol, 3-chloro- 31 3.60 3.80 4.00 4.20 m/z 82.95 5.39% 58 5000-

41

miz-> 0 TT-p-r-r-r-p-r 10 20 30 ..Ax 1.1.94 70 40 50 60 70 76

80 93 ■ ■ i ■ ■ • ■ i 1 • • ■ i 1 ■ ■ ‘ i ■ ■ ■ ■ i ■ 90 100 110 120 130 3.60 3.80 4.00 4.20

12763.D 060302.M. Mon Jun 10 10:29:04 2002 Page 10

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