GCMS sample AE12762 results, June 10 2002

NYC 9/11 Public Portal Document Library searen Compound Report

Data File C:\MSDCHEM\l\DATA\060702\12764.D Vial: 4 Acq On 7 Jun 2002 11:02 am Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Acetic acid, chloro-, ethyl... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.24 7.94 ug/L 4736040 1,4-dichlorobenzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 2 2 2-Chloroethanol 80 C2H5C10 000107-07-3 1 3 Piperidine, 2-propyl-, (S)- 127 C8H17N 000458-88-8 1 4 Pyrrolidine, 2-butyl-1-methyl- 141 C9H19N 003447-03-8 1 Abundance Scan 198 (4.243 min): 12764.D (-197) (-) m/z 49.10/ 100.00% 40

84 5000

38 73 3.80 4.00 4.20 4.40 4.60 0! ........... . Jili,,, 1 i ■ ' ■ ' i 1 — m/z 84.00 51.34% nz-> 10 20 30 40 50 60 70 90 100 80 110 120 130 Abundance #108005: Acetic acid, chloro-, ethyl ester 29

5000 3.80 4.00 4.20 4.40 4.60 77 42 49 m/z 86.00 39.29% 14

n/z-> 01 pl 10 20 +35 30 —40 11.59.95 50 60 .. 70 80 88 94 90 100 107 110 122 120 130 ++11 1 11 1 tti 11 । ri 11 । । 11 11 11 । । >

Abundance #108293: 2-Chloroethanol 31

3.80 4.00 4.20 4.40 4.60

niz-> 5000

01 -l10 20 30) 37 43 49 61 80 i ri । । 1-"t"s’u’n i i । i । i i । । i-i ifi । । । j । । । । । । । । । । । । । । । i । । i । । । 40 50 60 70 80 90 100 110 120 130 "Mwud, m/z 82.95 15.57%

Abundance #33701: Piperidine, 2-propyl-, (S)- 84 3.80 4.00 4.20 4.40 4.60 m/z 47.05 8.87%

5000

56 — .1 69 I 98 127 0 > ■ । >' 1 । । j । । । । । II—B—B—mm n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 3.80 4.00 4.20 4.40 4.60

12764.D 060302.M Mon Jun 10 10:30:00 2002 Page 11

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