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GCMS calibration results, June 11 2002

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Calibration verification data for volatile organic compound analysis using gas chromatography-mass spectrometry on June 11, 2002.

NYC-WTC_000015679–000015682

Folder label: “GCMS X 6/7/02 A 6/10/02

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NYC 9/11 Public Portal Document

Jser: Fakhouri, Morgan Vestchester Dept. of Labs & Research Jate: 06/11/2002 Time: 09:30:06

Sample: AE11933 Analysis: $C1GCMS CALI GCMS Jnits: ug Started: 6/11/02 09:22 Ended: 6/11/02 09:22 Analyst MF ’age: 1

Mads ~' Viol -Result- 1 Qualifier 'mpl i ; n-Nitrosodimethylamine ______ 15.80__________ 2.0 s bis(2-ChloroethyI)ether 17.12 2.0 .. 1,3-Dichlorobenzene 17.47 2.0 1,4-Dichlorobenzene 17.69_________ __________ 2.0________ t 1,2-Dichlorobenzene ______ 17.48__________ 2.0 th 2,2‘-oxybis(1 -Chloropropane) _____ 16.51__________ 2.0 n-Nitrosodi-n-propylamine ______ 16.14_________ __________ 2.0________ Hexachloroethane________ 17.14 2.0 4 Nitrobenzene 14.98 2.0 Isophorone ______ 16.13__________ __________ 2.0________ 1 bis(2-Chloroethoxy)methane ______ 16.56__________ __________ 2.0________ (28 1,2,4-Trichlorobenzene 17.44 2.0 3 Naphthalene___________ 17.72 2.0 Hexachlorobutadiene 18.21 2.0 2-Chloronaphthalene ______ 17.92__________ 2.0 Dimethylphthalate 16.88 2.0 2,6-Dinitrotoluene_______ 16.30 2.0 s Acenaphthylene ______ 18.51__________ __________ 2.0________ Acenaphthene ______ 18.25__________ __________ 2.0________ 2,4-Dinitrotoluene ______ 16.09__________ 2.0 Diethylphthalate ______ 17.80__________ __________ 2.0________ 4-Chlorophenylphenylether ______ 17.82__________ __________ 2.0________ | Fluorene 18.18 __________ 2.0________ | Azobenzene 17.56 2.0 ] n-Nitrosodiphenylamine 18.97 2.0 4-Bromophenyiphenylether [ Hexachlorobenzene ______ 18.09__________ _________ 2.0________ ______ 17.96__________ __________ 2.0________ [Phenanthrene ____ 18.41__________ 2.0 [Anthracene ______ 18.14__________ __________2.0________ | Dl-n-butylphthalate 13.77 2.0 [Fluoranthene 17.48 2.0 Pyrene ______ 16.59__________ 2.0 I Butylbenzylphthalate 15.84 2.0 | Benzo(a)anthracene ______ 14.97__________ 2.0 bis(2-Ethylhexyl)phthalate 16.18 2.0 Chrysene ____ 17.36_________ _ _________ 2.0________ Di-n-octylphthalate ______ 17.51__________ _________ 2.0________ Benzo(b)fluoranthene _____ 13.14__________ _________ 2.0________ Benzo(k)fluoranthene _____ 18.68__________ _________ 2.0________ Benzo(a)pyrene 14.80 2.0 lndeno(1,2,3-cd)pyrene _______7.26____________ 2.0 Dibenz(a,h)anthracene ______ 10.86__________ _________ 2.0________ Benzo(g,h,i)perylene 14.46 2.0

NYC-WTC_000015679

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