GCMS sample AE12761 results, June 10 2002

NYC 9/11 Public Portal Document Llbrary searcn compound Report

Data File C:\MSDCHEM\l\DATA\060602\12762.D Vial: 8 Acq On 6 Jun 2002 5:00 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L

Peak Number 4 1-Propanol, 3-chloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.78 2.60 ug/L 1856530 1 ,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanol, 3-chloro- 94 C3H7C1O 000627-30-5 2 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 3 Borane, trifluoro- 68 BF3 007637-07/ 1 4 2-Chloroethanol 80 C2H5C10 000107- -3 1 Abundance Scan 119 (3.779 min): 12762.D (-118) (-) m/z 4 9 .1 0 00.00% 49

5000

miz-> 0- 0 ....... 741...... 35

■ >i1■>■।■ > > >i>■।<i■<• । । ■ 10 20 30 40 50 60 । । 70 82 । . Nir 4,hpi 80 1 90 100 110 120 3.40 3.60 3.80 4.00 4.20 m/z 35.10 18.10% Abundance #108340:1-Propanol, 3-chloro- 31

58 5000 3.40 3.60 3.80 4.00 4.20 41 m/z 51.10 15.25% 76 0- 1TI 1 1 1 1 1 1 1 1411,1449.. TTHmT , 64 70 | , 93 ' i ■ ■ ■ 11 ■ 1 • ■ i ■ 1 ■ ■ i ■ ' niz-> o 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1082: Ethanol, 2,2-dichloro- 31

3.40 3.60 3.80 4.00 4.20 5000 m/z 41.10 9.80%

o- 25 , TITUII+T 37 43 49 55 61 70 77, 83 96 103 114 nz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #12321: Borane, trifluoro- 49 3.40 3.60 3.80 4.00 4.20 m/z 81.90 6.69% 5000

n/z—> 11 19 30 38 0- ■■1'I'■■■ i ■ ■ 1 ' I' ■ ■ ■ i ' ■ I ' ' ' ■ i 1 0 10 20 30 40 50 60 68 ** 70 80 90 100 110 120 Ah“WMMAynanan 3.40 3.60 3.80 4.00 4.20

12762.D 060302.M Mon Jun 10 10:26:33 2002 Page 7

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