GCMS reference standard results, June 10 2002

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Reference standard analysis report for volatile organic compounds using gas chromatography-mass spectrometry on June 10, 2002.

NYC-WTC_000015381–000015409

Folder label: “GCMS X 6/3/02 A 6/6/02”

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NYC 9/11 Public Portal Document Llbrary search compound Report

Data File C:\MSDCHEM\1\DATA\060602\12743.D Vial: 6 Acq On 6 Jun 2002 3:22 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 1,1,2-Trifluoroethane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.77 1.67 ug/L 1188490 1,4-dichlorob'enzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,2-Trifluoroethane 84 C2H3F3 000430-66-0 7 2 Propiolonitrile 51 C3HN 001070-71-9/5 3 Methane, chlorodifluoro- 86 CHC1F2 000075-45-6 1 4 Norflurane 102 C2H2F4 000811-97/2 1 Abundance Scan 118 (3.772 min): 12743.D (-116) (-) m/z 51.10 / 100.00% 51

5000 48 42 7275 84 38 340 3.60 3.80 4.00 4.20 01 010 • “ i"' ‘ i “ “ r " ' i' m/z 48.05 32.42% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12369:1,1,2-Trifluoroethane 51

5000 33 45 65 3.40 3.60 3.80 4.00 4.20 m/z 50.05 25.00%

miz-> 01-TH — — Tagu TTTTp-TTTp-rn

Abundance 19 26 69 8134 TT+++TTT^ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #12371: Propiolonitrile 51 MMMtry. • I ‘ ‘ - I ■ > - ■ I * ‘ ‘ ! i i > ■ j ■ 3.40 3.60 3.80 4.00 4.20 5000 m/z 42.05 19.58%

Ot 12 18 2528 32 38....47 ,....................... miz-> 5 10 15 20 25 30 35 40 45 50Hr55 60 65 70 75 80 85 90 95 T3 | I I I ! | 4 4 4 4 [T* 4 I | I I 4 4 J 4 1 4 4 | I 1 I I | 4 I 4 4 | I 4 4 4 I | 4 4 | 4 4 4 4 j 4 4 FT’ ITT I I I 1 | I I I I J J I J I | I I I I | J I I t | I I

Abundance #12363: Methane, chlorodifluoro- ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ ' ■ i ■ 51 3.40 3.60 3.80 4.00 4.20 m/ z 72.00 16.08% 5000

31 35 67 0 3131619 24 411111.38 r I t I ri 11111 111111111 47 —,54 11 Tpumanpantt ____ 70____ 8588 umpmmmmmp miz-s 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00 4.20

12743.D 060302.M Mon Jun 10 10:21:44 2002 Page 6

NYC-WTC_000015391

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