GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document LLOLCL DEcLCii topOUlU REDOL L

Data File C:\MSDCHEM\l\DATA\060702\12742.D Vial: 16 Acq On 7 Jun 2002 8:47 pm Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L Peak Number 3 Ethyl Chloride Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.82 1.09 ug/L 714178 1,4-dichlorob'enzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 2 2 2-Chloroethanol 80 C2H5C1O 000107-07-3/1 3 2-Chloroethanol 80 C2H5C10 000107-07-3 1 4 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38/9 1 Abundance Scan 126 (3.819 min): 12742.D (-125) (-) m/z 49.10 0.00% 40

5000 86 82 40 37 3.40 3.60 3.80 4.00 4.20 01 TTJT i ■ • ■' i " " r ' " i " " i ■"11' "I'"'I m/z 48.05 43.75% niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #107943: Ethyl Chloride 23 "WNo/ 64 5000 3.40 3.60 3.80 4.00 4.20 49 m/z 86.00 42.19% 25 35

Tl/Z-> O+ 5 10 15 20 25 30.......... 1215 TT TTHH ..... SI, 7........... . 35 40 45 50 55 60 65 70 75 80 85 90 I “ ‘' I' “ ‘ I “ " I ‘“ I' ‘" I'1' ‘ I

Abundance #108328:2-Chloroethanol 31 3.40 3.60 3.80 4.00 4.20 5000 m/z 81.90 25.39% 27 44 49 01 • • i ■ ■ ■ ■ i'1 ■ ■ i ■ ■ ■ ‘ i ■ ■ ■ ■ i ‘ .353841 ,153 576063 76 8° -f-r-t-l l} I i 1 i I i i > i I r I I 1 I i i i i I > j i i j 1 1 I 1 I t t i t I i i i i I > ! 1 1 I Masa n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #108291:2-Chloroethanol 31 3.40 3.60 3.80 4.00 4.20 m/z , ■ 47.00 21.29% 5000 ypt 15. 28 35 43 49 m/z-> 01 MHl 80 TTp—OTTDTTTTTTTWTTTTTITTTTTTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 3.40 3.60 3.80 4.00 4.20

12742.D 060302.M Mon Jun 10 11:26:24 2002 Page 6

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