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GCMS blank analysis report for sample AE12224, June 2002

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Laboratory report documenting a method blank analysis for GCMS testing of sample AE12224 to verify absence of contamination on June 3, 2002.

NYC-WTC_000015040–000015053

Folder label: “GCMS X 5/31/02 A 6/3/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\JUN0302\LB.D Vial: 3 Acq On 3 Jun 2002 10:40 am Operator: Morgan Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 14:28 2002 Quant Results File:GCMS0531 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.49 178 350 N.D. 36) Di-n-butylphthalate 27.41 149 4516 N.D. 3 7) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 29.81 202 171 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.48 228 2312 N.D. 42) Bis(2-ethylhexyl)phthalate 33.72 149 1914 N.D. 43) Chrysene 33.54 228 405 N.D. 45) Di-n-Octylphthalate 35.44 149 323 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.66 252 2599 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 41.74 278 186 N.D. 51) Benzo(g,h, i)perylene 42.84 276 875 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0531.M Mon Jun 03 14:28:46 2002 Page 2

NYC-WTC_000015042

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NYC-WTC_000015042Source: NYC Law Department, mirrored locally

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