GCMS analysis results for sample AE12576, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3102\12576.D Vial: 10 Acq On : 31 May 2002 8:51 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.07 0.62 ug/1 42337 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2.-Pentanone, 4-hydroxy-4-methyl - 116 C6H1202 000123-42-2 42 2 Guanidine 59 CH5N3 000113-00-8 9 3 3-Hexanol 102 C6H140 000623-37-0 9 4 2-Pentanol, 2,4-dimethyl - 116 C7H160 000625-06-9 9 Abundance Scan 330 (8.073 min): 12576.D (-) m/z 42.90 100.00% 43 59 5000- t

101 nmnnm—torrrmmr 7.80 8.00 8.20 8.40 51 8? ....... 11000711111113, Ipanapnnji TTo 711' “11' m/z 59.00 57.44% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 PAp/i 7.80 8.00 8.20 8.40 rn/ Z 58.00 21.07% 15 31 101 83 mmm Tpth m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 TT Abundance #100: Guanidine 43 59 1 ‘ ■ i ■ ■ ■ ■ i f ■ i ‘ ■ i ’ 1 1 ■ 7.80 8.00 8.20 8.40 5000 m/z 101.05 20.50%

17 31

.... K..... q - tanasqanaqqaal tmmmmmmmmmmmmmmmp HT W m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63531:3-Hexanol 59 7.80 8.00 8.20 8.40 m/z 40.90 6.25% 5000 73

43

miz—> mmmHHHmmpm - 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 .A4.A4.4.., 7.80 8.00 8.20 8.40

12576.D GCMS0531.M Mon Jun 03 09:35:18 2002 Page 1

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