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GCMS analysis results, sample AE12151, June 2002

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis report for sample AE12151, completed on 6/6/02 at 14:58, testing for unknown compounds and 2,4-DDD surrogate.

NYC-WTC_000014902–000014911

Folder label: “GCMS X 5/29/02 A 5/31/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\MAY3102\12151.D Vial: 8 Acq On : 31 May 2002 6:52 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P 2"* Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) rres Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC . peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 8.072 326 330 343 rBV 24922 66898 1.80% 0.322% 2 12.065 760 765 789 rBV 1069853 2638194 71.01% 12.716% 3 15.691 1154 1160 1179 rBV 1617048 3583255 96.45% 17.271% 4 20.997 1730 1738 1757 rBV 1696818 3687911 99.27% 17.775% 5 23.136 1962 1971 1977 rBV 943971 1980080 53.30% 9.544% 6 25.432 2214 2221 2231 rBV 1768595 3715192 100.00% 17.906% 7 25.569 2232 2236 2248 rVB 13398 44174 1.19% 0.213% 8 33.483 3090 3098 3118 rBV2 1185183 2858841 76.95% 13.779% 9 37.660 3545 3553 3569 rBV2 744320 2173223 58.50% 10.474%

Sum of corrected areas: 20747768 12151.D GCMS0531.M Mon Jun 03 09:34:42 2002

NYC-WTC_000014907

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NYC-WTC_000014907Source: NYC Law Department, mirrored locally

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